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Reaction id: 0210291027_32, verified by Personal Chemistry ©
1303
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530
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BMimPF6
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product 28
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Yield: N/A Time: 900s Temperature: 240 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 589082 |
135.210 |
0.930 |
3.439 |
500.000 µl |
| 93583 |
136.150 |
1.094 |
0.434 |
54.000 µl |
| BMimPF6 |
284.184 |
1.000 |
0.352 |
100.000 µl |
| Product 1 |
239.318 |
1.000 |
0.000 |
0.000 µl |
Keywords
Amidation, Aminolysis
Comments
Synthesis: See also entries 0206241010 and 0207031014 for experimental data.
Work up: The reaction mixture was suspended in 2 ml of ethylacetate and filtered before analysis.
Purification: No further purification was made for this substrate.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Wuensch, B.; Hoefner, G.; Bauschke, G.; Heterocycles [HTCYAM] 1990, 31 (8), 1427-1429
Analysis
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0210291027_32A.pdf