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Reaction id: 0207031014_03, verified by Personal Chemistry ©
912
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1205
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BMimPF6
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P3
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Yield: 85% Time: 900s Temperature: 240 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 3770501 |
189.214 |
1.000 |
0.499 |
94.469 mg |
| 91214 |
133.194 |
1.064 |
3.994 |
500.000 µl |
| BMimPF6 |
284.184 |
1.000 |
0.352 |
100.000 µl |
| Product 1 |
276.339 |
1.000 |
0.499 |
137.893 mg |
Keywords
Amidation, Aminolysis
Comments
Purification: The reaction mixture was suspended in 1.5 ml of ethyl acetate, filtered, and purified by chromatography on silica, ethyl acetate:heptane, 1:1, giving colourless crystals.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Wuensch, B.; Hoefner, G.; Bauschke, G. Heterocycles 1990, 31 (8), 1427-1429
Analysis
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0207031014_03A.pdf