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Reaction id: 0210251021_04, verified by Personal Chemistry ©
1123
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NH4OH
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Product 4
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Yield: N/A Time: 600s Temperature: 150 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 286-20-4 |
98.145 |
0.970 |
1.000 |
101.180 µl |
| NH4OH |
35.046 |
1.000 |
68.448 |
2398.820 µl |
| Product 1 |
115.176 |
0.970 |
1.000 |
118.738 µl |
Keywords
Addition, Amination, Ring opening, SN2, Substitution
Comments
Synthesis: This type of reaction does not work out so good, if the epoxide is sterically hindered.
Work-up: The reaction mixture was extracted with 3.0 ml methylene chloride and the aqeous phase was analysed by GCMS.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Lindström, U. M.; Olofsson B.; Somfai, P. Tetrahedron Letters 1999, 40, 9273-9276
Analysis
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0210251021_04G.pdf