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Pathfinder Cookbook - reaction details
Reaction id: 0211141023_10, verified by Personal Chemistry ©

12

957

1401
Acetic acid

P10

Yield: N/A  Time: 300s   Temperature: 180 °C

Chemicals
 Name MW [g/mol] Density [g/ml] Amount [mmol] Mass/Volume
631618 77.083 1.000 1.500 115.624 mg
492944 190.154 1.000 0.500 95.077 mg
446526 124.114 1.178 0.500 52.680 µl
Acetic acid 60.052 1.050 34.970 2000.000 µl
Product 1 294.285 1.000 0.500 147.142 µl

Keywords
Heterocyclic, Multicomponent

Comments
Work-up: The reaction mixture was filtered through a syringe filter.

Purification: The reaction mixture was purified using preparative RP-LCMS.

Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s

References
Usyatinsky, A. Y.; Khmelnitsky, Y. L. Tet. Lett. 2000, 41, 5031-5034 Balalaie, S.; Arabanian, A. Green Chem. 2000, 2, 274-276 Balalaie, S.; Arabanian, A.; Hashtroudi, M.S. Monatshefte für Chemie Chemical Monthly 2000, 131, 945-948

Analysis
 Method Purity Files
 crude LCMS 66  0211141023_10A.pdf
 1H NMR  0211141023_10N_H.pdf