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Reaction id: 0211181011_08, verified by Personal Chemistry ©
883
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MeSO3H
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Product 5
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Yield: N/A Time: 40s Temperature: 160 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 19501587 |
174.631 |
1.000 |
0.700 |
122.242 mg |
| MeSO3H |
96.104 |
1.482 |
12.337 |
800.002 µl |
| Product 1 |
124.143 |
1.000 |
0.700 |
86.900 mg |
Keywords
Demethylation, Deprotection
Comments
Synthesis: At 120°C and shorter reaction times less starting material was converted to product. Longer reaction times, up to 180 s, did not alter the conversion pattern for this substrate.
Instrument Settings
Absorption level: High
Pre-stirring time: 0s
References
Fredriksson, A.; Stone-Elander, S. J. Label. Compd. Radiopharm. 2002, 45, 529-538
Analysis
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0211181011_08A.pdf