|
|  |
Reaction id: 0210171021_08, verified by Personal Chemistry ©
250
|
|
773
|
|
|
 |
1,4-Dioxane
water
|
|
P2
|
Yield: N/A Time: 300s Temperature: 160 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 603-35-0 |
262.292 |
1.000 |
3.300 |
865.563 mg |
| 23095-31-0 |
236.673 |
1.000 |
0.500 |
118.336 mg |
| 1,4-Dioxane |
88.106 |
1.000 |
28.375 |
2500.000 µl |
| water |
18.015 |
1.000 |
27.755 |
500.000 µl |
| Product 1 |
170.230 |
1.000 |
0.000 |
0.000 mg |
Keywords
Reduction, S-Deoxygenation
Comments
Analysis: The product did not ionize in APCI but showed an UV-spectrum identical to the isolated product from the reaction with PS-supported triphenylphosphine.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Ko, K.-Y.; Kim, K.-I.; Bull. Korean. Chem. Soc. 1998, 19(3), 378-379
Analysis
|
|
|
|
|
0210171021_08A.pdf