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Reaction id: 0210171021_07, verified by Personal Chemistry ©
250
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774
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1,4-Dioxane
water
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P1
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Yield: N/A Time: 300s Temperature: 160 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 603-35-0 |
262.292 |
1.000 |
3.300 |
865.563 mg |
| 605-65-2 |
269.750 |
1.000 |
0.500 |
134.875 mg |
| 1,4-Dioxane |
88.106 |
1.000 |
28.375 |
2500.000 µl |
| water |
18.015 |
1.000 |
27.755 |
500.000 µl |
| Product 1 |
203.307 |
1.000 |
0.000 |
0.000 mg |
Keywords
Reduction, S-Deoxygenation
Comments
Analysis: The product was chromatographically identical with the isolated product from the reaction with PS-supported triphenylphosphine.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Ko, K.-Y.; Kim, K.-I.; Bull. Korean. Chem. Soc. 1998, 19(3), 378-379
Analysis
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0210171021_07A.pdf