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Reaction id: 0211201017_17, verified by Personal Chemistry ©
1272
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143
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1,2-Dichloroethane
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P8
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Yield: N/A Time: 600s Temperature: 200 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 556821 |
86.134 |
0.848 |
2.500 |
253.933 µl |
| 1313139 |
86.936 |
1.000 |
3.000 |
260.808 mg |
| 1,2-Dichloroethane |
98.960 |
1.000 |
25.263 |
2500.000 µl |
| Product 1 |
84.118 |
1.000 |
2.500 |
210.295 µl |
Keywords
Oxidation
Comments
Analysis: LCMS showed a purity of 95 % at 254 nm and a strong molecular ion of 85 was detected, which unfortunately is not clearly seen in the attached MS. A Crude NMR of the product was not possible due to the low bp. of the produced aldehyde.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Firouzabadi, H.; Karimi, B.; Abbassi, M. J. Chem. Res. 1999, 236
Analysis
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0211201017_17A.pdf