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Reaction id: 0210091013_12, verified by Personal Chemistry ©
1017
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966
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Piperidine
Acetic acid
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EtOH
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P12
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Yield: N/A Time: 1500s Temperature: 180 °C
Chemicals
| Name |
MW [g/mol] |
Density [g/ml] |
Amount [mmol] |
Mass/Volume |
| 487898 |
145.161 |
1.000 |
0.500 |
72.581 mg |
| 96568046 |
280.082 |
1.000 |
0.600 |
168.049 mg |
| Piperidine (0.5M in THF) |
85.150 |
1.000 |
0.100 |
200.000 µl |
| Acetic acid (0.5M in THF) |
60.052 |
1.000 |
0.100 |
200.000 µl |
| EtOH |
46.069 |
1.000 |
45.584 |
2100.000 µl |
| Product 1 |
407.228 |
1.000 |
0.500 |
203.614 mg |
Keywords
Knoevenagel Condensation
Comments
Synthesis: The reaction was also performed with DMF as solvent at the same temp./time conditions, but then the reaction mixture contained more impurities.
Instrument Settings
Absorption level: Normal
Pre-stirring time: 0s
References
Kuster, G.J.; Scheeren, H.W., Tetrahedron Lett. (2000), 515-519
Analysis
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0210091013_12A.pdf